articleTop 10% cited
Structural order in MCM-41 controlled by shifting silicate polymerization equilibrium
Journal of the Chemical Society Chemical Communications · 1995 · pp. 711–711
Abstract
Powder X-ray diffraction, 29Si and 129Xe NMR spectroscopy of MCM-41 show that the long-range structural order and textural uniformity of the mesoporous molecular sieve are markedly improved due to a shift in the reaction equilibrium when acetic acid is repeatedly added during the conversion of sodium silicate and NMe3(C16H33)Cl to a MCM-41 phase.
Mesoporous Materials and CatalysisZeolite Catalysis and SynthesisMetal-Organic Frameworks: Synthesis and ApplicationsMolecular sieveSilicatePolymerizationSodium silicateChemistryMesoporous materialAcetic acidMCM-41Nuclear magnetic resonance spectroscopyPowder diffraction
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References
A new family of mesoporous molecular sieves prepared with liquid crystal templates
Journal of the American Chemical Society · 1992 · 10,852 citations
Ordered mesoporous molecular sieves synthesized by a liquid-crystal template mechanism
Nature · 1992 · 16,077 citations
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