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Calibration Curve for Quantitative Analysis of the Monoclinic-Tetragonal ZrO<sub>2</sub>System by X-Ray Diffraction
Journal of the American Ceramic Society · 1984 · Vol. 67(6) · pp. C–119
H. Toraya✉(Tokyo Institute of Technology)Masahiro Yoshimura(Tokyo Institute of Technology)Shigeyuki Sōmiya(American Ceramic Society)
Abstract
A nonlinear calibration curve for volume fraction vs integrated intensity ratio was obtained for the monoclinic-tetragonal ZrO2 system by using X-ray powder pattern-fitting and pattern-decomposition techniques. The empirical equation agrees well with the theoretical one. By using this equation, the deviation from linearity (6.8% maximum) resulting from the intensity difference of corresponding reflections of the two phases can be estimated quite accurately.
X-ray Diffraction in CrystallographyFerroelectric and Piezoelectric MaterialsNuclear materials and radiation effectsMonoclinic crystal systemTetragonal crystal systemDiffractionIntensity (physics)CalibrationX-ray crystallographyCalibration curveLinearityMaterials scienceX-ray
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817
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Cited by
Quantitative Analysis of Monoclinic‐Stabilized Cubic ZrO <sub>2</sub> Systems by X‐Ray Diffraction
Journal of the American Ceramic Society · 1984 · 832 citations
References
A profile refinement method for nuclear and magnetic structures
Journal of Applied Crystallography · 1969 · 17,034 citations
Phase Analysis in Zirconia Systems
Journal of the American Ceramic Society · 1972 · 1,419 citations
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